On May 21, 2008, Zhu, Renfa published a patent.Product Details of 38838-06-1 The title of the patent was Method for synthesizing 1,2,3-O-triacetyl-5-deoxy-D-ribofuranose. And the patent contained the following:
The title method comprises adopting D-ribose as raw material, performing glycosidation and esterification to obtain 2,3-O-isopropylidene-5-O-p-toluenesulfonyl-D-ribofuranose, performing iodination with sodium iodide or potassium iodide to obtain 2,3-O-isopropylidene-5-iodo-5-deoxy-D-ribofuranose, performing catalytic hydrogenation to obtain 2,3-O-isopropylidene-5-deoxy-D-ribofuranose, and hydrolyzing to obtain the final product with m.p. of 62-64°C. The method has the advantages of mild reaction condition, wide raw material resources, no pollution, and high yield (37.8%). The experimental process involved the reaction of (3aS,4S,6R,6aR)-4-(Iodomethyl)-6-methoxy-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxole(cas: 38838-06-1).Product Details of 38838-06-1
The Article related to deoxyribofuranose triacetate preparation green chem, Carbohydrates: Glycosides and other aspects.Product Details of 38838-06-1
Referemce:
1,3-Benzodioxole – Wikipedia,
Dioxole | C3H4O2 – PubChem