Lu, Baolan’s team published research in Jingxi Shiyou Huagong Jinzhan in 12 | CAS: 177-10-6

Jingxi Shiyou Huagong Jinzhan published new progress about 177-10-6. 177-10-6 belongs to dioxole, auxiliary class Dioxolane,Spiro, name is 1,4-Dioxaspiro[4.5]decane, and the molecular formula is C8H14O2, Formula: C8H14O2.

Lu, Baolan published the artcileCatalytic synthesis of cyclohexanone ethylene ketal over phosphotungstic acid/silica gel, Formula: C8H14O2, the publication is Jingxi Shiyou Huagong Jinzhan (2011), 12(12), 50-52, database is CAplus.

Cyclohexanone ethylene ketal I was synthesized with cyclohexanone and glycol as the materials, and the catalytic activity of phosphotungstic acid/silica gel catalyst in ketol reaction was studied. According to the results, phosphotungstic acid/silica gel (SG) is a good catalyst for the synthesis of cyclohexanone ethylene ketal. The optimum synthesis conditions were identified: n (cyclohexanone):n (glycol) = 1:1.4, amount of water-carrying agent (i.e. cyclohexane): 8 mL, reaction time: 30 min. The yield of cyclohexanone ethylene ketal can reach 76.4% at such conditions.

Jingxi Shiyou Huagong Jinzhan published new progress about 177-10-6. 177-10-6 belongs to dioxole, auxiliary class Dioxolane,Spiro, name is 1,4-Dioxaspiro[4.5]decane, and the molecular formula is C8H14O2, Formula: C8H14O2.

Referemce:
https://en.wikipedia.org/wiki/1,3-Benzodioxole,
Dioxole | C3H4O2 – PubChem