Downstream synthetic route of 4,5-Dimethyl-1,3-dioxol-2-one

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4725 g of dichloroethane was added to the DMDO that was stirred up.1012.5g N-chlorosuccinimideAnd 45g benzoyl peroxide,Reaction temperature 90¡ãC, reaction time 5.5h,The crude product obtained DMDO-Cl 382.5g, a yield of 85.00percent; Step 3: Distillation: The DMDO-Cl crude product at -0.1MPa vacuum,Distilled at 110¡ãC to produce 326g of DMDO-ClThe purity by gas chromatography was 99.06percent.

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Reference£º
Patent; Puyang Tianyuan Biological Technology Co., Ltd.; Zhao Junxia; Wen Jiaogang; Wang Lixia; Lv Xiaoyong; Fu Jingchao; Liu Renhuan; Chen Yongzhuang; Wang Lina; (6 pag.)CN107892681; (2018); A;,
1,3-Benzodioxole – Wikipedia
Dioxole | C3H4O2 – PubChem