Downstream synthetic route of 4,5-Dimethyl-1,3-dioxol-2-one

With the synthetic route has been constantly updated, we look forward to future research findings about 4,5-Dimethyl-1,3-dioxol-2-one,belong Dioxole compound

As a common heterocyclic compound, it belongs to quinuclidine compound,Quinuclidine-4-carboxylic acid hydrochloride,40117-63-3,Molecular formula: C8H14ClNO399,mainly used in chemical industry, its synthesis route is as follows.,37830-90-3

Example 17 Preparation of 5-methyl-4-hydroxymethyl-2-oxo-1,3-dioxolene A solution of 4,5-dimethyl-2-oxo-1,3-dioxolene (1 mmol) and selenium dioxide (2.5 mmol) in dioxane was heated at reflux for 1 h. Evaporation, extraction and chromatography gave 5-methyl-4-hydroxymethyl-2-oxo-1,3-dioxolene as a yellow oil. TLC: Rf=0.5, 5percent MeOH-dichloromethane.

With the synthetic route has been constantly updated, we look forward to future research findings about 4,5-Dimethyl-1,3-dioxol-2-one,belong Dioxole compound

Reference£º
Patent; Metabasis Therapeutics, Inc.; US6284748; (2001); B1;,
1,3-Benzodioxole – Wikipedia
Dioxole | C3H4O2 – PubChem