Preparation of fructone from ethyl acetoacetate and ethylene glycol in the presence of copper benzenesulfonate as catalyst was written by Dong, Jing-hua. And the article was included in Huagong Jishu Yu Kaifa in 2013.Related Products of 6413-10-1 The following contents are mentioned in the article:
Fructone was prepared by condensation reaction of Et acetoacetate and ethylene glycol in the presence of copper benzene sulfonate. The influences of the reaction conditions on the yield of fructone were investigated. The optimum reaction conditions were as follows: molar ratio of Et acetoacetate/ethylene glycol, 1:1.5; catalyst dosage, 1.5wt% of reactants; water-carrying agent, cyclohexane; reaction time, 60min. Under the optimum reaction conditions, the yield of fructone was up to 82.7%. This study involved multiple reactions and reactants, such as Ethyl 2-(2-methyl-1,3-dioxolan-2-yl)acetate (cas: 6413-10-1Related Products of 6413-10-1).
Ethyl 2-(2-methyl-1,3-dioxolan-2-yl)acetate (cas: 6413-10-1) belongs to dioxole derivatives. Dioxoles, particularly fluorinated dioxoles, are used as co-monomers to make polymers that find use in forming protective coatings for chemical resistance. Dioxole functionalized metal-organic frameworks have also been recently reported.Related Products of 6413-10-1
Referemce:
1,3-Benzodioxole – Wikipedia,
Dioxole | C3H4O2 – PubChem