A new synthetic route of 4,5-Dimethyl-1,3-dioxol-2-one

A chemical reaction often occurs in steps, although it may not always be obvious to an observer.

An elementary termolecular reaction involves the simultaneous collision of three atoms, molecules, or ions.4,5-Dimethyl-1,3-dioxol-2-one, cas is 37830-90-3. Here is a downstream synthesis route of the compound 37830-90-3, 37830-90-3

A mixture of 4,5-dimethyl-1,3-dioxol-2-one (1.0 g, 8.8 mmol), benzoylperoxide (60 mg, 0.25 mmol) and N-bromosuccinimide (1.6 g, 9.0 mmol) in carbon tetrachloride (10 mL) was heated at reflux for 2 h. The solid was removed from the reaction mixture by filtration. The mother liquid was washed with sat. NaHCO3 and brine, dried over MgSO4 and concentrated. The crude product, 4-(bromomethyl)-5-methyl-1,3-dioxol-2-one, was obtained as a yellow oil (1.7 g) and was used without further purification in the next step.

A chemical reaction often occurs in steps, although it may not always be obvious to an observer.

Reference£º
Patent; Martinsson, Jessica; Faernegardh, Katarina; Joensson, Mattias; Ringom, Rune; US2015/25068; (2015); A1;,
1,3-Benzodioxole – Wikipedia
Dioxole | C3H4O2 – PubChem