Yang, Shuijin published the artcileCatalytic synthesis of cyclohexanone ethylene ketal with H3PW12O40/TiO2-SiO2, Application In Synthesis of 177-10-6, the publication is Jingxi Shiyou Huagong Jinzhan (2014), 15(6), 48-50, 54, database is CAplus.
Cyclohexanone and ethylene glycol were used to synthesize cyclohexanone ethylene ketal with H3PW12O40/TiO2-SiO2 as the catalyst which was prepared with method of impregnation. The effects of the molar ratio of cyclohexanone to ethylene glycol, catalyst usage, and reaction time on the yield were studied in experiment The results of experiment have shown that H3PW12O40/TiO2-SiO2 is a good catalyst for the synthesis of cyclohexanone ethylene ketal. The optimum synthesis conditions were identified : n (cyclohexanone) : n (ethylene glycol) = 1 : 1.4, catalyst usage is 0.8% of the total mass of reaction materials, and the usage of cyclohexane, i.e. the water carrying agent, is 6 mL. The yield of cyclohexanone ethylene ketal reaches 77.6% at such conditions.
Jingxi Shiyou Huagong Jinzhan published new progress about 177-10-6. 177-10-6 belongs to dioxole, auxiliary class Dioxolane,Spiro, name is 1,4-Dioxaspiro[4.5]decane, and the molecular formula is C8H16N2O, Application In Synthesis of 177-10-6.
Referemce:
https://en.wikipedia.org/wiki/1,3-Benzodioxole,
Dioxole | C3H4O2 – PubChem