Li, Ruiyun published the artcileEfficient and reusable SBA-15-immobilized Bronsted acidic ionic liquid for the ketalization of cyclohexanone with glycol, Synthetic Route of 177-10-6, the publication is RSC Advances (2018), 8(13), 7179-7185, database is CAplus and MEDLINE.
Ketalization of cyclohexanone with glycol has been carried out using mol. sieve SBA-15 immobilized Bronsted acidic ionic liquid catalyst. The properties of the heterogeneous catalysts were characterized by elemental anal., Fourier transform IR spectra, SEM, thermogravimetry/differential scanning calorimetry, and N2 adsorption-desorption. The results suggested that Bronsted acidic ionic liquid [BSmim][HSO4] had been successfully immobilized on the surface of SBA-15 and the catalytic performance evaluation demonstrated that the catalyst BAIL@SBA-15 exhibited excellent catalytic activities in the ketalization of cyclohexanone with glycol. In addition, the effects of reaction temperature, catalyst loading, reaction time, and reactant molar ratio have also been investigated in detail, and a general reaction mechanism for the ketalization of cyclohexanone with glycol was given. The SBA-15 immobilized ionic liquid can be recovered easily and after reusing for 5 times in the ketalization reaction, the catalyst could still give satisfactory catalytic activity.
RSC Advances published new progress about 177-10-6. 177-10-6 belongs to dioxole, auxiliary class Dioxolane,Spiro, name is 1,4-Dioxaspiro[4.5]decane, and the molecular formula is C8H14O2, Synthetic Route of 177-10-6.
Referemce:
https://en.wikipedia.org/wiki/1,3-Benzodioxole,
Dioxole | C3H4O2 – PubChem