Synthetic Route of C34H22NO2P. Aromatic heterocyclic compounds can also be classified according to the number of heteroatoms contained in the heterocycle: single heteroatom, two heteroatoms, three heteroatoms and four heteroatoms. Compound: 5-(11bR)-Dinaphtho[2,1-d:1′,2′-f][1,3,2]dioxaphosphepin-4-yl-5H-dibenz[b,f]azepine, is researched, Molecular C34H22NO2P, CAS is 1265884-98-7, about Iridium-catalyzed enantioselective synthesis of (-)- and (+)-aurantioclavine. Author is Lei, Ting; Zhang, Hongbin; Yang, Yu-Rong.
A new protocol for generating indoleazepine I via an Ir-catalyzed intramolecularly asym. amination of secondary allylic alc. II in the presence of Carreira ligand and Sc(OTf)3 is described. This methodol. has been exploited in the facile synthesis of natural (-)-aurantioclavine (III), a biosynthetical precursor of communesins, and its unnatural enantiomer (+)-aurantioclavine (ent-III).
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Reference:
1,3-Benzodioxole – Wikipedia,
Dioxole | C3H4O2 – PubChem