Continuously updated synthesis method about 4,5-Dimethyl-1,3-dioxol-2-one

Elementary reactions that involve the simultaneous collision of more than three molecules are highly improbable and have never been observed experimentally.

Rate laws may be derived directly from the chemical equations for elementary reactions. This is not the case, however, for ordinary chemical reactions.37830-90-3, molecula formula is 4,5-Dimethyl-1,3-dioxol-2-one, below Introduce a new synthetic route., 37830-90-3

To a solution of 16 grams 4,5-dimethyl-1, 3-dioxol-2-one in CC14 (250 mE) was added N135 (23.4 g,131.5 mmol) and AII3N (1.3 g, 7.88 mmol), then the reaction mixture was heated to 80¡ã C. and stirred for 2 hrs. Monitored the starting material gone by TLC. The mixture was filtered and the filtrate was washed with water and brine, the organic phase was dried over Na2504 and concentrated to give crude product as a yellow oil which was used directly next step (25.3 g, yield 93percent).

Elementary reactions that involve the simultaneous collision of more than three molecules are highly improbable and have never been observed experimentally.

Reference£º
Patent; KULING THERAPEUTICS; DING, Qiang; Wang, Xiaohu; (55 pag.)US2017/298090; (2017); A1;,
1,3-Benzodioxole – Wikipedia
Dioxole | C3H4O2 – PubChem